CoSAXS beamline at MAX IV: optical design and sample environment for advanced SAXS/WAXS applications

TUP14
16 Sept 2025, 17:00
1h
Poster Session Room (The Loop)

Poster Session Room

The Loop

Poster Presentation Beamlines and Instruments Tuesday Poster Session

Speaker

Matheus Da Silva (MAX IV Laboratory)

Description

CoSAXS is a versatile SAXS/WAXS beamline at the 3 GeV diffraction-limited ring of MAX IV Laboratory in Sweden. The optical design [$*$ ,$**$] delivers X-ray beams from 4–20 keV with 0.01% bandwidth and photon flux of 10¹²–10¹³ ph/s, with up to 10% coherent flux at 7.1 keV. Beam sizes at the sample range from 250 × 250 μm² to 30 × 15 μm² (FWHM). The SAXS detector (Eiger2 4M) moves longitudinally and transversely inside a 15 m vacuum vessel. The fixed WAXS detector (Pilatus3) is positioned at the vessel entrance, and a Mythen2 1K in air provides 1D WAXS. The q-range spans ~6 × 10⁻⁴ to 3 Å⁻¹ (d-spacings: 1 μm–2 Å). Supported techniques include solution and solid SAXS/WAXS, SEC/AF4-SAXS [$*******$], USAXS, TRSS in the ms range [$***$, $****$], and coherent scattering [$*****$]. Sample environments include magnetic fields, rheology, biaxial stretching [$******$], and microfluidics [$********$]. Control and data systems are described in [$****$]. After nearly 5 years of operation, CoSAXS has completed 190 proposals, including 19 proprietary research projects. The beamline has a high demand and has contributed to 47 publications.

Footnotes

$*$ A.J. Allen, J. Appl. Cryst. 56, 787 (2023)
$**$ T.S. Plivelic, et al. AIP Conf. Proc. 2054, 030013 (2019)
$***$ O. Berntsson, et al. J. Synchrotron Rad. 29, 555 (2022)
$****$ V. Silva, et al. JACoW ICALEPCS2023 713 (2023)
$*****$ M. Kahnt, et al. J. Synchrotron Rad. 28 1948 (2022)
$******$ P. Mota-Santiago, et al. J. Appl. Cryst. 56 967 (2023)
$*******$ H. Bolinsson, et al Anal. Bioanal. Chem. 415, 6237 (2023)
$********$ J. Gilbert, et al. J. Colloid Interface Sci 660, 66 (2024)

Author

Matheus Da Silva (MAX IV Laboratory)

Co-authors

Ann Terry (MAX IV Laboratory) Byungnam Ahn (MAX IV Laboratory) Fatima Herranz Trillo (MAX IV Laboratory) Jackson Luis Da Silva (MAX IV Laboratory) Marcelo Alcocer (MAX IV Laboratory) Marco Leorato (MAX IV Laboratory) Raul Barrea (Benedictine University) Roberto Appio (MAX IV Laboratory) Tomás Plivelic (MAX IV Laboratory) Vanessa Da Silva (MAX IV Laboratory)

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